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Analysis of HPLC Coupled with Tandem Mass Spectrometry (HPLCMS/MS) Optimization of the Mobile Phase The first mobile phases were methanol (solvent A) and water (solvent B) in a linear gradient from 0% to 15 % of methanol over 5 min, with the isocratic stage holding at 15 % methanol for 5 min

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Native amylin is co-secreted with insulin after meals and signals satiety, slows gastric emptying, and blunts post-meal glucagon